Jan 22 2019 The direct impregnation of PIM-1 with MIL-101Cr powder by physical mixing in tetrachloroethane solvent can readily lead to cross-linked PIM-1MIL-101Cr monolith bodies. This was achieved by preparing separate tetrachloroethane-based solutions of PIM-1 and suspension of various loadings of pre-dried MIL-101Cr powder 40 60 and 80 wt.
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Dec 15 2018 The precursor powder MIL-53Fe or NH 2-MIL-53Fe was placed in a tube furnace and then heated to the required temperature for 3 h at a heating rate of 5 Cmin under a flowing nitrogen atmosphere 25 5 mLmin. After cooling to room temperature the black powder
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Sep 01 2020 The morphology and particle size of as-prepared MIL-88AFe were investigated by SEM and TEM images. As illustrated in Fig. 1 the pristine MIL-88AFe displayed uniform and well-crystallized hexagonal micro-rods with an average size of 7001200 nm in length and 200400 nm in diameter which was slightly smaller than those in the previous reports Huang et al. 2018 Liu et al. 2018a Liu .
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